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Generally, tetramethylethylenediamine, (TMEDA), improved the yield of products, and it was necessary for the successful condensation of the lithiated ester-sulfonamide with dilithiated alpha-acetyl-gamma-butyrolactone, even though the yield was 36%.
Supplies two aromatic amines, DMP-10 and DMP-30, as well as tetramethylethylenediamine as epoxy curing agents.
The effect of tetramethylethylenediamine, (TMEDA), on the yields of products will be presented along with relevant spectral characterization of new 3-substituted aryl 4,5-dihydronaphth[1,2-c]isoxazoles and 1-subsituted aryl 4,5-dihydro-[2,1-c]isoxazoles.
Tetramethylethylenediamine and fresh ammonium persulfate were added immediately before pouring.